Издательство СО РАН

Издательство СО РАН

Адрес Издательства СО РАН: Россия, 630090, а/я 187
Новосибирск, Морской пр., 2

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Яндекс.Метрика

Поиск по журналу

Журнал структурной химии

2016 год, номер 5

CHARACTERIZATION, LUMINESCENT PROPERTIES, CRYSTAL STRUCTURE DETERMINATION, AND THERMAL PROPERTIES OF [Tl(Ph2phen)Cl3(DMSO)]

M. Ghadermazi
University of Kurdistan, Sanandaj, Iran
mghadermazi@yahoo.com
Ключевые слова: synthesis, Tl(III), 4,7-diphenyl-1,10-phenanthroline, crystal structure, thermal gravimetric, differential thermal analysis, luminescent properties
Страницы: 1020-1025

Аннотация

The new mixed-ligand complex of [Tl(Ph2phen)Cl3(DMSO)] (1) is obtained from the reaction of TlCl3×4H2O with 4,7-diphenyl-1,10-phenanthroline (Ph2phen) in a methanol solution. Suitable crystals of 1 are obtained for the X-ray diffraction measurement by methanol diffusion into a DMSO solution. This complex is characterized by spectral methods (IR, UV-Vis, 1H NMR, and luminescence), elemental analysis, thermal analysis (TG, DTA), and single crystal X-ray diffraction.

DOI: 10.15372/JSC20160517
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