Издательство СО РАН

Издательство СО РАН

Адрес Издательства СО РАН: Россия, 630090, а/я 187
Новосибирск, Морской пр., 2

soran2.gif

Baner_Nauka_Sibiri.jpg


Яндекс.Метрика

Array
(
    [SESS_AUTH] => Array
        (
            [POLICY] => Array
                (
                    [SESSION_TIMEOUT] => 24
                    [SESSION_IP_MASK] => 0.0.0.0
                    [MAX_STORE_NUM] => 10
                    [STORE_IP_MASK] => 0.0.0.0
                    [STORE_TIMEOUT] => 525600
                    [CHECKWORD_TIMEOUT] => 525600
                    [PASSWORD_LENGTH] => 6
                    [PASSWORD_UPPERCASE] => N
                    [PASSWORD_LOWERCASE] => N
                    [PASSWORD_DIGITS] => N
                    [PASSWORD_PUNCTUATION] => N
                    [LOGIN_ATTEMPTS] => 0
                    [PASSWORD_REQUIREMENTS] => Пароль должен быть не менее 6 символов длиной.
                )

        )

    [SESS_IP] => 54.234.6.167
    [SESS_TIME] => 1711709428
    [BX_SESSION_SIGN] => 9b3eeb12a31176bf2731c6c072271eb6
    [fixed_session_id] => db5e1c97dc34045010df374f39c33741
    [UNIQUE_KEY] => d8dc252c44aff1b0a5ac7f065afa68c9
    [BX_LOGIN_NEED_CAPTCHA_LOGIN] => Array
        (
            [LOGIN] => 
            [POLICY_ATTEMPTS] => 0
        )

)

Поиск по журналу

Химия в интересах устойчивого развития

2005 год, номер 2

Mechanochemically Assisted Synthesis of Bi2Mo3O12 Catalysts

D. Klissurski, D. Radev, R. Iordanova and M. Milanova
Institute of General and Inorganic Chemistry, Bulgarian Academy of Sciences,
G. Bonchev str., bl. 11, 1113 Sofia (Bulgaria), E-mail: dklis@igic.bas.bg
Страницы: 225-228

Аннотация

The solid phase synthesis of Bi2Mo3O12 is investigated. The mechanochemical activation is used in order to reduce the synthesis times and temperatures. A 5 h mechanical treatment leads to a drastic decrease in the temperature of classical solid state synthesis of Bi2Mo3O12 (from 600 to 350oC). The product obtained is single-phase, consisting of even size distributed submicronic particles. The synthesis of Bi2Mo3O12 was monitored by X-ray diffraction (XRD) and infrared spectroscopy (IR). Shape and size changes of reagent particles after mechanical treatment and morphological peculiarities of the products were studied by SEM.